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Wednesday, October 27, 2010

ICE THAT BURNS

20 OCTOBER 2010
where things get hawt.




Is it a hot figure skater on ice?


NO.

But This.


UPCLOSE WITH SUPERCOOLING OF SODIUM ACETATE

Sodium acetate or hot ice is an amazing chemical you can prepare from baking soda and vinegar. Cooling of sodium acetate solution below its melting point will cause the liquid to crystallize. The crystallization is an exothermic process, so the resulting ice is hot.

Alternatively, Sodium thiosulphate-5-water could be used.

Apparatus and chemicals:

Boiling Tube

Stirring Thermometer

Beaker (100cm3)

Bunsen Burner

Tripod and wire gauze

Sodium acetate crystals

Hows its done:

The apparatus is set up and sodium acetate is left to melt in a water bath into a clear liquid. This process takes about 20-30minutes for the water to vapourise completely.

The sodium acetate solution is then left to cool in a beaker of iced water.

(If the liquid does start to crystallise,it is reheated to melt all the solid once more.)

Observe that at 30-40 degree Celcius, crystallization should not occur.

Add a fresh crystal of sodium acetate (drop it in the solution)and observe rapid crystallization occuring.

:) TADAA


Everyone had the patience of a monk, awaiting the melting of sodium acetate crystals. Go people!



Setting the apparatus up.




Reo Sei adjusting the height :)








The meeting ended about 4.45pm. Most of our sodium acetate crystallized before we even touch it, but ofcourse, some succeeded in this experiment too. The main key is to cover the boiling tube to prevent foreign particles to enter and freeze it.





And yes, the ice was burning hot.

:D






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